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Photolabeling of TGR with PRP TGR (1 µM) or SmHDAC8 (1 µM) was incubated at concentrations of either 5 or 50 µM PRP with or without 100 µM NADPH totaling eight samples

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HILIC separation was performed using a Waters BEH Amide column (100 mm × 2.1 mm, 1.7 μm)